Angadi Institute of Technology and Management, India
The unique features of
reduced graphene oxide (rGO) enable their applications in the field of
photocatalysis as well as unique electrical properties. In the present research
work, a novel series of Nb doped CeO2 decorated with rGO (2, 8 and
12 wt %) were synthesized by hydrothermal method. The structural and
morphological features of nanomaterials (NMs) investigated by using different
analytical techniques namely, XRD (X-ray diffraction), UV-visible, SEM
(scanning electron microscopy), EDX (energy dispersive X-ray), XPS (X-ray
photoelectron spectroscopy), BET (Brunauer-Emmett-Teller).
The XRD analysis present polycrystalline mixed phase of tetragonal/cubic
crystal structure and microstructure analysis showed flower shaped morphology
having mesoporous nature. The addition of rGO results in the increased specific
surface area and pore diameter. Redshift in optical absorbance results with
decrease in direct optical band gap as rGO concentration increases in NMs. The
EDX/XPS studies showed the chemical composition and oxidation states of
elements NB, Ce, O, C in NMs. Zeta potential studies showed increased poly
disparity with increase in the mobility of the NMs. The zeta potential varies
from 88.1 mV to 110.8 mV as the rGO concentration increases on bimetallic oxide
NMs. Further, Photocatalytic dye degradation studies of rGO (2, 8 and 12 wt %): Nb2O3@CeO2
against Methylene blue (NM), Rodhamaine B (RB) and Sudan 1 dye showed increased
photocatalytic activity. The Photocatalytic performances increase with increase
in rGO concentration on bimetallic oxide NMs. The findings of the present work can
be better candidate for photocatalytic and an excellent material for charge
transport capability.
Fifteen years of research experience as senior Scientist, associate research scientist in R&D organizations of TATA, Astra Zeneca India, Trans Chem Ltd. Overseas Research Fellow of Nanyang Global Research Center, Bangkok, Malaysia. Published more than 150 research articles, and 15 Books/several book chapters in Scopus, Q-ratted journals with high impact factor, attended and presented papers in National and International Conferences as Key note speaker, distinguished speaker, Chaired/ Key note speaker/Organizing secretory, Editor for International and National conferences, Editorial Board Member, Life Member of many international societies. Editor of the special issues published in springer, Elsevier and Wiley. Research interest includes, Optoelectronics, Material Chemistry, Sensors and Actuators, Bio Nanomaterials, Medicinal Chemistry.